The synthesis and characterization of novel porphyrazines containing 5H-dibenz[b,f]azepine units
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Abstract
The synthesis of novel metal-free (H2Pz) and metalloporphyrazines (MgPz), peripherally substituted with eight 5H-dibenz[b,f]azepine was performed by the cyclotetramerization of 1,5-bis(dibenz[b,f]azepinepropylthio)maleonitrile which was synthesized from 5H-dibenz[b,f]azepine and 1,10-diiodo-5,6-dicyano-4,7-dithia-5-decene. The new compounds were characterized by elemental analysis, 1H NMR, 13C NMR, IR, UV-vis and mass spectral data. © 2007.
Description
Keywords
Dibenzazepine, Magnesium, Metal-free porphyrazine, Porphyrazinatomagnesium, Template effect, Characterization, Chemical analysis, Porphyrins, Synthesis (chemical), Porphyrazine, Dyes, infrared radiation, magnetic resonance imaging, organic compound, synthesis, ultraviolet radiation, 570, ultraviolet radiation, Porphyrins, organic compound, synthesis, Porphyrazinatomagnesium, Characterization, Porphyrazine, Template effect, Dibenzazepine, 540, Metal-free porphyrazine, Synthesis (chemical), magnetic resonance imaging, Magnesium, Chemical analysis, infrared radiation, Dyes
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01 natural sciences, 0104 chemical sciences
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77
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2
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351
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356
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