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https://hdl.handle.net/11499/10949
Title: | Gold nanoparticles/two-dimensional (2D) hexagonal boron nitride nanosheets including diethylstilbestrol imprinted polymer: Electrochemical detection in urine samples and validation | Authors: | Yola, M.L. Atar, Necip |
Keywords: | Boron nitride Cyclic voltammetry Electrochemical impedance spectroscopy Fiber optic sensors Glass membrane electrodes Gold nanoparticles III-V semiconductors Metal nanoparticles Nanosheets Nitrides Phenols Scanning electron microscopy Transmission electron microscopy X ray photoelectron spectroscopy Detection limits ELectrochemical detection Glassy carbon electrodes Hexagonal boron nitride Imprinted polymers Linearity range Natural estrogen Two Dimensional (2 D) Chemical detection |
Publisher: | Electrochemical Society Inc. | Abstract: | A new diethylstilbestrol (DES) imprinted sensor approach based on gold nanoparticles (AuNPs) incorporated two-dimensional (2D) hexagonal boron nitride (2D-hBN) nanosheets was presented for DES detection. The methods such as scanning electron microscope (SEM), transmission electron microscope (TEM), X-ray photoelectron spectroscopy (XPS), X-ray diffraction (XRD) method, cyclic voltammetry (CV) and electrochemical impedance spectroscopy (EIS) were used for all nanomaterials’ characterizations. DES imprinted sensor was prepared in presence of 100.0 mM pyrrole containing 25.0 mM DES by CV. The developed method was validated and 5.0 x 10-12-1.0 x 10-8 M and 1.0 x 10-13 M were founded as the linearity range and the detection limit (LOD). DES imprinted glassy carbon electrode (GCE) was applied in presence of the natural estrogens such as estrone (E1), estradiol (E2) and estriol (E3) and the other agents such as hydroquinone (HYD) and catechol (CAT). © 2018 The Electrochemical Society. | URI: | https://hdl.handle.net/11499/10949 https://doi.org/10.1149/2.0421814jes |
ISSN: | 0013-4651 |
Appears in Collections: | Mühendislik Fakültesi Koleksiyonu Scopus İndeksli Yayınlar Koleksiyonu / Scopus Indexed Publications Collection WoS İndeksli Yayınlar Koleksiyonu / WoS Indexed Publications Collection |
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