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https://hdl.handle.net/11499/30523
Title: | Synthesis, crystal structure, spectroscopic features and Hirshfeld surfaces of 2-methyl-3-[(2-methylphenyl) carbamoyl]phenyl acetate | Authors: | Yaman, M. Cakmak, Ş. Dege, N. Odabaşoglu, Mustafa Pavlenko, V.A. Kutuk, H. |
Keywords: | amide crystal structure Hirshfeld surface hydrogen bonding. X-ray diffraction |
Publisher: | International Union of Crystallography | Abstract: | The title compound, C17H17NO3, was synthesized, characterized by IR spectroscopy and its crystal structure was determined from single-crystal diffraction data. The asymmetric unit contains two molecules, which adopt different conformations. In one molecule, the acetoxy and the terminal 2-methylphenyl groups are positioned on opposite sides of the plane formed by the central benzene ring, whereas in the other molecule they lie on the same side of this plane. In the crystal, the molecules are linked through strong N-H O hydrogen bonds into chains along [010]. Hirshfeld surface analysis and fingerprint plots were used to investigate the intermolecular interactions in the solid state. © 2019 International Union of Crystallography. All rights reserved. | URI: | https://hdl.handle.net/11499/30523 https://doi.org/10.1107/S2056989019000021 |
ISSN: | 2056-9890 |
Appears in Collections: | Denizli Teknik Bilimler Meslek Yüksekokulu Koleksiyonu PubMed İndeksli Yayınlar Koleksiyonu / PubMed Indexed Publications Collection Scopus İndeksli Yayınlar Koleksiyonu / Scopus Indexed Publications Collection WoS İndeksli Yayınlar Koleksiyonu / WoS Indexed Publications Collection |
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synthesis.pdf | 1.17 MB | Adobe PDF | View/Open |
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