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Title: | Synthesis and characterization of a new (E,E)-dioxime and its homonuclear complexes | Authors: | Karapınar, Emin | Keywords: | BF2+ - capped complex Crown compounds Glyoximes Transition metal complexes |
Abstract: | N'-(4'-Benzo[15-crown-5]naphthylaminoglyoxime (H2L) and its sodium chloride complex (H2L·NaCl) have been prepared from 2-naphthylchloroglyoxime, 4'-aminobenzo[15-crown-5] and sodium bicarbonate or sodium bicarbonate and sodium chloride. Nickel(II), cobalt(II) and copper(II) complexes of H2L and H2L·NaCl have a metal-ligand ratio of 1:2 and the ligand coordinates through the two N atoms, as do most of the vic-dioximes. The BF 2 + -capped Ni(II), Co(III) and mononuclear complexes of thevic-dioxime were prepared. The macrocyclic ligands and their transition metal complexes have been characterized on the basis of IR, 1H NMR spectroscopy and elemental analyses data. © Springer 2005. | URI: | https://hdl.handle.net/11499/4766 https://doi.org/10.1007/s10847-005-2548-z |
ISSN: | 0923-0750 |
Appears in Collections: | Fen-Edebiyat Fakültesi Koleksiyonu Scopus İndeksli Yayınlar Koleksiyonu / Scopus Indexed Publications Collection WoS İndeksli Yayınlar Koleksiyonu / WoS Indexed Publications Collection |
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