Please use this identifier to cite or link to this item: https://hdl.handle.net/11499/51064
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dc.contributor.authorÖzgür, Ayşe-
dc.contributor.authorAktürk, Ezgi Zekiye-
dc.contributor.authorKöseoğlu, Denizcan-
dc.contributor.authorOnaç, Canan-
dc.contributor.authorAkdoğan, Abdullah-
dc.date.accessioned2023-06-13T19:08:11Z-
dc.date.available2023-06-13T19:08:11Z-
dc.date.issued2023-
dc.identifier.issn0889-1575-
dc.identifier.issn1096-0481-
dc.identifier.urihttps://doi.org/10.1016/j.jfca.2023.105208-
dc.identifier.urihttps://hdl.handle.net/11499/51064-
dc.description.abstractA sensitive and efficient green emulsification liquid-liquid microextraction (ELLME) method using deep eutectic solvents (DES) for extraction of phthalates released from food contact materials (FCMs) was optimized for GC-MS determination of Butyl Benzyl Phthalate (BBP) and Di-2-Ethylhexyl Phthalate (DEHP). The optimal DES system for phthalate extraction was determined to be Choline Chloride:Phenol (1:2 molar ratio). Tetrahydrofuran (THF) was utilized as the emulsifier solvent. The effects of vortex agitation times and centrifugation times on extraction efficiency were investigated. The method yielded quantification limits (LOQ) of 0.036 and 0.005 mgL-1 for BBP and DEHP, respectively. Repeatability relative standard deviations (RSDr) of 2.9% and 2.2% were obtained for BBP and DEHP, respectively, while corresponding medium precision relative standard deviations (RSDR) were 2.8% and 3.2%. Recovery rates from spiked samples were 94.8% for BBP and 95.1% for DEHP. Finally, deter-mination of BBP and DEHP released from contact materials into water and beverage samples at various tem-peratures confirmed the applicability of the method for assessment of phthalates and their migration from FCMs.en_US
dc.description.sponsorshipUnit of the Scientific Research Projects of Pamukkale University [2019FEBE003]en_US
dc.description.sponsorshipThe authors are grateful for the financial support of the Unit of the Scientific Research Projects of Pamukkale University (2019FEBE003) (Denizli,Turkiye) .en_US
dc.language.isoenen_US
dc.publisherAcademic Press Inc Elsevier Scienceen_US
dc.relation.ispartofJournal of Food Composition and Analysisen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectPhthalatesen_US
dc.subjectDeep Eutectic Solventen_US
dc.subjectGreen solventen_US
dc.subjectEmulsification liquid-liquid microextractionen_US
dc.subjectGas chromatographyen_US
dc.subjectFood contact materialsen_US
dc.subjectFood analysisen_US
dc.subjectFood compositionen_US
dc.subjectLiquid-Liquid Microextractionen_US
dc.subjectSolid-Phase Extractionen_US
dc.subjectEnvironmental Wateren_US
dc.subjectBottled Wateren_US
dc.subjectMigrationen_US
dc.subjectEstersen_US
dc.subjectPolyethyleneen_US
dc.subjectSpectrometryen_US
dc.subjectMicrowaveen_US
dc.subjectRemovalen_US
dc.titleDeep Eutectic Solvent-based green extraction and gas chromatography determination of phthalates released from food contact materialsen_US
dc.typeArticleen_US
dc.identifier.volume118en_US
dc.departmentPamukkale Universityen_US
dc.identifier.doi10.1016/j.jfca.2023.105208-
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.authorscopusid58156437500-
dc.authorscopusid58155959100-
dc.authorscopusid58155478800-
dc.authorscopusid55660205800-
dc.authorscopusid6602909512-
dc.identifier.scopus2-s2.0-85150814049en_US
dc.identifier.wosWOS:000939849800001en_US
dc.institutionauthor-
dc.identifier.scopusqualityQ1-
item.cerifentitytypePublications-
item.fulltextNo Fulltext-
item.grantfulltextnone-
item.openairecristypehttp://purl.org/coar/resource_type/c_18cf-
item.languageiso639-1en-
item.openairetypeArticle-
crisitem.author.dept01.04. Centre For Advanced Research Laboratory-
crisitem.author.dept17.01. Chemistry-
Appears in Collections:Mühendislik Fakültesi Koleksiyonu
Scopus İndeksli Yayınlar Koleksiyonu / Scopus Indexed Publications Collection
WoS İndeksli Yayınlar Koleksiyonu / WoS Indexed Publications Collection
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