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https://hdl.handle.net/11499/51064
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DC Field | Value | Language |
---|---|---|
dc.contributor.author | Özgür, Ayşe | - |
dc.contributor.author | Aktürk, Ezgi Zekiye | - |
dc.contributor.author | Köseoğlu, Denizcan | - |
dc.contributor.author | Onaç, Canan | - |
dc.contributor.author | Akdoğan, Abdullah | - |
dc.date.accessioned | 2023-06-13T19:08:11Z | - |
dc.date.available | 2023-06-13T19:08:11Z | - |
dc.date.issued | 2023 | - |
dc.identifier.issn | 0889-1575 | - |
dc.identifier.issn | 1096-0481 | - |
dc.identifier.uri | https://doi.org/10.1016/j.jfca.2023.105208 | - |
dc.identifier.uri | https://hdl.handle.net/11499/51064 | - |
dc.description.abstract | A sensitive and efficient green emulsification liquid-liquid microextraction (ELLME) method using deep eutectic solvents (DES) for extraction of phthalates released from food contact materials (FCMs) was optimized for GC-MS determination of Butyl Benzyl Phthalate (BBP) and Di-2-Ethylhexyl Phthalate (DEHP). The optimal DES system for phthalate extraction was determined to be Choline Chloride:Phenol (1:2 molar ratio). Tetrahydrofuran (THF) was utilized as the emulsifier solvent. The effects of vortex agitation times and centrifugation times on extraction efficiency were investigated. The method yielded quantification limits (LOQ) of 0.036 and 0.005 mgL-1 for BBP and DEHP, respectively. Repeatability relative standard deviations (RSDr) of 2.9% and 2.2% were obtained for BBP and DEHP, respectively, while corresponding medium precision relative standard deviations (RSDR) were 2.8% and 3.2%. Recovery rates from spiked samples were 94.8% for BBP and 95.1% for DEHP. Finally, deter-mination of BBP and DEHP released from contact materials into water and beverage samples at various tem-peratures confirmed the applicability of the method for assessment of phthalates and their migration from FCMs. | en_US |
dc.description.sponsorship | Unit of the Scientific Research Projects of Pamukkale University [2019FEBE003] | en_US |
dc.description.sponsorship | The authors are grateful for the financial support of the Unit of the Scientific Research Projects of Pamukkale University (2019FEBE003) (Denizli,Turkiye) . | en_US |
dc.language.iso | en | en_US |
dc.publisher | Academic Press Inc Elsevier Science | en_US |
dc.relation.ispartof | Journal of Food Composition and Analysis | en_US |
dc.rights | info:eu-repo/semantics/closedAccess | en_US |
dc.subject | Phthalates | en_US |
dc.subject | Deep Eutectic Solvent | en_US |
dc.subject | Green solvent | en_US |
dc.subject | Emulsification liquid-liquid microextraction | en_US |
dc.subject | Gas chromatography | en_US |
dc.subject | Food contact materials | en_US |
dc.subject | Food analysis | en_US |
dc.subject | Food composition | en_US |
dc.subject | Liquid-Liquid Microextraction | en_US |
dc.subject | Solid-Phase Extraction | en_US |
dc.subject | Environmental Water | en_US |
dc.subject | Bottled Water | en_US |
dc.subject | Migration | en_US |
dc.subject | Esters | en_US |
dc.subject | Polyethylene | en_US |
dc.subject | Spectrometry | en_US |
dc.subject | Microwave | en_US |
dc.subject | Removal | en_US |
dc.title | Deep Eutectic Solvent-based green extraction and gas chromatography determination of phthalates released from food contact materials | en_US |
dc.type | Article | en_US |
dc.identifier.volume | 118 | en_US |
dc.department | Pamukkale University | en_US |
dc.identifier.doi | 10.1016/j.jfca.2023.105208 | - |
dc.relation.publicationcategory | Makale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı | en_US |
dc.authorscopusid | 58156437500 | - |
dc.authorscopusid | 58155959100 | - |
dc.authorscopusid | 58155478800 | - |
dc.authorscopusid | 55660205800 | - |
dc.authorscopusid | 6602909512 | - |
dc.identifier.scopus | 2-s2.0-85150814049 | en_US |
dc.identifier.wos | WOS:000939849800001 | en_US |
dc.institutionauthor | … | - |
dc.identifier.scopusquality | Q1 | - |
item.cerifentitytype | Publications | - |
item.fulltext | No Fulltext | - |
item.grantfulltext | none | - |
item.openairecristype | http://purl.org/coar/resource_type/c_18cf | - |
item.languageiso639-1 | en | - |
item.openairetype | Article | - |
crisitem.author.dept | 01.04. Centre For Advanced Research Laboratory | - |
crisitem.author.dept | 17.01. Chemistry | - |
Appears in Collections: | Mühendislik Fakültesi Koleksiyonu Scopus İndeksli Yayınlar Koleksiyonu / Scopus Indexed Publications Collection WoS İndeksli Yayınlar Koleksiyonu / WoS Indexed Publications Collection |
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