Please use this identifier to cite or link to this item: https://hdl.handle.net/11499/5353
Title: Determination of some trace metals in waters by flame atomic absorption spectrometry after preconcentration on amberlite XAD-16 resin with sodium tetraborate
Authors: Tokalioglu, S.
Kartal, Ş.
Elçi, Latif
Keywords: Amberlite XAD 16
Amberlite XAD-16
heavy metal
ion exchange resin
polymer
sea water
article
atomic absorption spectrometry
human
methodology
sewage
water pollutant
water supply
Humans
Ion Exchange Resins
Metals, Heavy
Polymers
Seawater
Spectrophotometry, Atomic
Waste Disposal, Fluid
Water Pollutants, Chemical
Water Supply
Abstract: A method was described for the determination of the elements Cr, Mn, Fe, Co, Ni, Cu, Cd, Pb, and Bi in waters by flame atomic absorption spectrometry (FAAS) after separation and preconcentration on Amberlite XAD-16 resin with sodium tetraborate using a Chromatographic column. Parameters influencing the analytical performance, including pH and the volume of sample, amount of analyte and interfering effect of co-existing ions, were studied in detail. The recovery values were quantitative (? 95 %), and the relative standard deviation (RSD) and detection limit (DL) varied in the range of 1.1-2.4 % (n=10) and 0.002-0.177 µg ml-1 (3s, n=20), respectively. After being optimized, the proposed method was applied to the drinking water, waste water and artificial sea water samples. Recovery values of the elements investigated, were quantitative for tap water and synthetic sea water, except for Mn, Co and Ni (including also Cd for synthetic sea water). Recovery values of Cd, Pb, Cu and Co were found to be 95, 102, ?87, and ?83%, respectively, for the waste water samples.
URI: https://hdl.handle.net/11499/5353
ISSN: 0003-4592
Appears in Collections:Fen-Edebiyat Fakültesi Koleksiyonu
PubMed İndeksli Yayınlar Koleksiyonu / PubMed Indexed Publications Collection
Scopus İndeksli Yayınlar Koleksiyonu / Scopus Indexed Publications Collection
WoS İndeksli Yayınlar Koleksiyonu / WoS Indexed Publications Collection

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