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https://hdl.handle.net/11499/5421
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DC Field | Value | Language |
---|---|---|
dc.contributor.author | Karatepe, A.U. | - |
dc.contributor.author | Soylak, M. | - |
dc.contributor.author | Elçi, Latif | - |
dc.date.accessioned | 2019-08-16T11:46:48Z | |
dc.date.available | 2019-08-16T11:46:48Z | |
dc.date.issued | 2002 | - |
dc.identifier.issn | 0003-2719 | - |
dc.identifier.uri | https://hdl.handle.net/11499/5421 | - |
dc.identifier.uri | https://doi.org/10.1081/AL-120006731 | - |
dc.description.abstract | A simple enrichment method for trace amounts of Cu(II), Fe(III), Pb(II), Co(II) and Cr(III) has been established. The preconcentration/separation procedure is based on chelate formation of the analyte metals with benzopurpurine 4B and on retention of the chelates on cellulose nitrate membrane filter. After completely dissolving the cellulose nitrate membrane and analyte ions by 500 µL of nitric acid at 85°C on a hood, metal determinations were performed by flame atomic absorption spectrometry. The influences of some analytical parameters including pH, types of membrane filters, amounts of reagent etc. on the recoveries of copper, iron, lead, cobalt and chromium were investigated. The detection limits of the analyte ions (k=3, N=21) were varying 1.9 µg/L for cobalt to 10.5 µg/L for iron. The method was applied to natural water samples for the determination of analyte ions with satisfactory results (recoveries > 95%, RSD < 10%). The relative standard deviations (RSD) of the determinations for analyte ions were below 10%. | en_US |
dc.language.iso | en | en_US |
dc.relation.ispartof | Analytical Letters | en_US |
dc.rights | info:eu-repo/semantics/closedAccess | en_US |
dc.subject | Cellulose nitrate membrane | en_US |
dc.subject | FAAS | en_US |
dc.subject | Natural water samples | en_US |
dc.subject | Preconcentration | en_US |
dc.subject | Separation | en_US |
dc.subject | chromium | en_US |
dc.subject | cobalt | en_US |
dc.subject | copper | en_US |
dc.subject | iron | en_US |
dc.subject | lead | en_US |
dc.subject | pyroxylin | en_US |
dc.subject | analytic method | en_US |
dc.subject | aqueous solution | en_US |
dc.subject | article | en_US |
dc.subject | atomic absorption spectrometry | en_US |
dc.subject | flame atomic absorption spectrometry | en_US |
dc.subject | membrane filter | en_US |
dc.subject | pH | en_US |
dc.subject | spectrometry | en_US |
dc.subject | water analysis | en_US |
dc.subject | water sampling | en_US |
dc.title | Separation/preconcentration of Cu(II), Fe(III), Pb(II), Co(II), and Cr(III) in aqueous samples on cellulose nitrate membrane filter and their determination by atomic absorption spectrometry | en_US |
dc.type | Article | en_US |
dc.identifier.volume | 35 | en_US |
dc.identifier.issue | 9 | en_US |
dc.identifier.startpage | 1561 | |
dc.identifier.startpage | 1561 | en_US |
dc.identifier.endpage | 1574 | en_US |
dc.identifier.doi | 10.1081/AL-120006731 | - |
dc.relation.publicationcategory | Makale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı | en_US |
dc.identifier.scopus | 2-s2.0-0036354507 | en_US |
dc.identifier.wos | WOS:000177716700010 | en_US |
dc.identifier.scopusquality | Q2 | - |
dc.owner | Pamukkale_University | - |
item.openairetype | Article | - |
item.grantfulltext | none | - |
item.cerifentitytype | Publications | - |
item.fulltext | No Fulltext | - |
item.languageiso639-1 | en | - |
item.openairecristype | http://purl.org/coar/resource_type/c_18cf | - |
crisitem.author.dept | 17.01. Chemistry | - |
Appears in Collections: | Fen-Edebiyat Fakültesi Koleksiyonu Scopus İndeksli Yayınlar Koleksiyonu / Scopus Indexed Publications Collection WoS İndeksli Yayınlar Koleksiyonu / WoS Indexed Publications Collection |
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