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https://hdl.handle.net/11499/58215
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DC Field | Value | Language |
---|---|---|
dc.contributor.author | Perveen, Saima | - |
dc.contributor.author | Hol, Aysen | - |
dc.contributor.author | Baig, Jameel Ahmed | - |
dc.contributor.author | Sherazi, Syed Tufail Hussain | - |
dc.contributor.author | Akhtar, Khalil | - |
dc.contributor.author | Hussain, Sajjad | - |
dc.contributor.author | Abbasi, Fahad | - |
dc.date.accessioned | 2024-11-20T18:03:31Z | - |
dc.date.available | 2024-11-20T18:03:31Z | - |
dc.date.issued | 2024 | - |
dc.identifier.issn | 0267-9477 | - |
dc.identifier.issn | 1364-5544 | - |
dc.identifier.uri | https://doi.org/10.1039/d4ja00210e | - |
dc.identifier.uri | https://hdl.handle.net/11499/58215 | - |
dc.description.abstract | In the current study, a solid phase extraction (SPE) methodology utilizing sodium ferrite nanoparticles (Na2Fe4O7-NPs; SF-NPs) is presented for the simultaneous determination of heavy metals (HMs) via flame atomic absorption spectrometry (FAAS). SF-NPs were synthesized by an eco-friendly sol-gel auto-combustion method using Tamarindus indica fruit extract as a stabilizing agent. The characterized SF-NPs exhibited a high surface area with uniform distribution, high stability, and a negative surface charge, making it a promising material for excellent adsorption of HMs. The SF-NP-based SPE procedure involved optimizing parameters such as pH, adsorbent dosage, sample volume, eluent composition, volume, and concentration. The developed SF-NP-based SPE method demonstrated low detection limits, i.e., 0.006, 0.008, and 0.009 mu g L-1 for the analysis of Cd, Cu, and Pb, respectively. The SF-NP-based SPE methodology was validated by examining certified reference material and real samples, yielding accurate results with good recoveries (>95%) with a relative standard deviation of <5.0%. The developed SF-NP-based SPE method offers a promising approach for the simultaneous determination of Cd, Cu, and Pb in water and food samples, providing an efficient and environmentally friendly analytical tool for monitoring heavy metal contamination. | en_US |
dc.description.sponsorship | Chemistry Department, Pamukkale University, Denizli, Turkey; National Centre of Excellence in Analytical Chemistry, University of Sindh, Jamshoro-PAKISTAN | en_US |
dc.description.sponsorship | The authors thank the Chemistry Department, Pamukkale University, Denizli, Turkey and the National Centre of Excellence in Analytical Chemistry, University of Sindh, Jamshoro-PAKISTAN, for their support in the current experimental activities. Their funding has been influential in the present study's success and paved the way for further discoveries and exploration. | en_US |
dc.language.iso | en | en_US |
dc.publisher | Royal Soc Chemistry | en_US |
dc.relation.ispartof | Journal of Analytical Atomic Spectrometry | en_US |
dc.rights | info:eu-repo/semantics/closedAccess | en_US |
dc.subject | Preconcentration | en_US |
dc.subject | Separation | en_US |
dc.subject | Food | en_US |
dc.title | Sodium nanoferrite-based solid phase extraction: a green method for the simultaneous determination of cadmium, copper, and lead | en_US |
dc.type | Article | en_US |
dc.identifier.volume | 39 | en_US |
dc.identifier.issue | 11 | en_US |
dc.identifier.startpage | 2884 | en_US |
dc.identifier.endpage | 2892 | en_US |
dc.department | Pamukkale University | en_US |
dc.authorid | HOL, AYSEN/0000-0002-7883-2435 | - |
dc.authorid | Hussain, Sajjad/0000-0001-6145-0484 | - |
dc.authorid | Baig, Jameel Ahmed/0000-0002-4338-9103 | - |
dc.identifier.doi | 10.1039/d4ja00210e | - |
dc.relation.publicationcategory | Makale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı | en_US |
dc.authorscopusid | 58714992200 | - |
dc.authorscopusid | 23492566500 | - |
dc.authorscopusid | 35565546600 | - |
dc.authorscopusid | 14827378900 | - |
dc.authorscopusid | 57373839500 | - |
dc.authorscopusid | 57755755500 | - |
dc.authorscopusid | 57456164600 | - |
dc.authorwosid | Baig, Jameel/X-6041-2019 | - |
dc.authorwosid | Perveen, Saima/HTL-9894-2023 | - |
dc.authorwosid | Hussain, Sajjad/IST-9107-2023 | - |
dc.authorwosid | Sherazi, Syed Tufail/J-5321-2019 | - |
dc.authorwosid | HOL, AYSEN/HKE-3610-2023 | - |
dc.authorwosid | Baig, Jameel Ahmed/P-1481-2018 | - |
dc.identifier.scopus | 2-s2.0-85206210816 | en_US |
dc.identifier.wos | WOS:001330737500001 | en_US |
dc.institutionauthor | … | - |
item.languageiso639-1 | en | - |
item.openairetype | Article | - |
item.openairecristype | http://purl.org/coar/resource_type/c_18cf | - |
item.fulltext | No Fulltext | - |
item.grantfulltext | none | - |
item.cerifentitytype | Publications | - |
crisitem.author.dept | 17.01. Chemistry | - |
Appears in Collections: | Fen Fakültesi Koleksiyonu Scopus İndeksli Yayınlar Koleksiyonu / Scopus Indexed Publications Collection WoS İndeksli Yayınlar Koleksiyonu / WoS Indexed Publications Collection |
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