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Title: Diazolu ve schiff bazlı kaliks[4]aren bileşikleri ve metal kompleksleri
Other Titles: Calix[4]arena compounds with diazo and schiff base and metal complexes
Authors: Zencir, Sevil
Advisors: Emin Erdem
Keywords: Kaliks[4]aren
Schiff Bazları
Kaliks[4]aren Metal Kompleksleri
Azo boyarmadde
Schiff Base
Calix[4]arene Metal Complexes
Azo Dyes
Publisher: Pamukkale Üniversitesi Fen Bilimleri Enstitüsü
Abstract: Bu çalışmada diazo ve Schiff bazı grubu bulunduran p-(2-hidroksi, 3-metoksi fenil imin fenilazo)kaliks[4]aren (SB1) ve p-(2-hidroksi, fenil imin fenilazo)kaliks[4]aren (SB2) ligandları ve bu ligandların Ni2+, Cu2+ ve Co2+ kompleksleri sentezlendi. Ligandların ve 1 komplekslerin yapıları H-NMR, IR, UV-VIS, DTA-TG, AAS, LC-MS ve Magnetik süsseptibilite teknikleri ile araştırıldı.
In this study, p-(2-hydroxy, 3-methoxy phenyl imine phenylazo)calix[4]arene (SB1) and p- (2-hydroxy, phenyl imine phenylazo)calix[4]arene (SB2) ligands which have diazo and Schif base groups and their Ni2+, Cu2+ ve Co2+ complexes were synthesized. Structure of the ligands and complexes were investigated by 1H-NMR, IR, UV-VIS, DTA-TG, AAS, LC-MS, Magnetic süsceptibility techniques.
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